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Year/Semester of Study | 1 / Fall Semester | ||||
Level of Course | 3rd Cycle Degree Programme | ||||
Type of Course | Optional | ||||
Department | TEKLİF EDİLEN KIMYA (DOKTORA) | ||||
Pre-requisities and Co-requisites | None | ||||
Mode of Delivery | Face to Face | ||||
Teaching Period | 14 Weeks | ||||
Name of Lecturer | ASLIHAN UZUN (akaratepe@nevsehir.edu.tr) | ||||
Name of Lecturer(s) | |||||
Language of Instruction | Turkish | ||||
Work Placement(s) | None | ||||
Objectives of the Course | |||||
The aim of this course is to teach students information about proving the suitability of a method or measurement procedure for the purposes determined with written evidence by objective testing. |
Learning Outcomes | PO | MME | |
The students who succeeded in this course: | |||
LO-1 | Can know what method validation is and why it is needed. |
PO-1 Develop advanced theoretical and applied knowledge in the field, depending on undergraduate and graduate qualifications. PO-3 Can closely follow national and international developments in the field of chemistry. PO-4 Can systematically follow up-to-date information in the field. PO-6 Can has a scientific and professional ethical understanding and can defend this understanding in any environment. PO-7 Can develop new ideas and methods with different perspectives by using high-level competencies such as suggesting solutions to problems that arise in the field and making decisions. PO-8 Can design theoretical, experimental, or modeling-based research that will contribute to progress in the field, develop new scientific methods, and apply a known method to a different field. PO-9 Can produce solutions to social, scientific, and ethical issues by combining their own knowledge and perspective with up-to-date information about their field. |
Examination |
LO-2 | Can know the parameters used in method validation. |
PO-1 Develop advanced theoretical and applied knowledge in the field, depending on undergraduate and graduate qualifications. PO-2 Can make connections between different disciplines and sub-fields that their field is related to by using their expert knowledge and skills, work in harmony in research groups. PO-3 Can closely follow national and international developments in the field of chemistry. PO-4 Can systematically follow up-to-date information in the field. PO-7 Can develop new ideas and methods with different perspectives by using high-level competencies such as suggesting solutions to problems that arise in the field and making decisions. PO-8 Can design theoretical, experimental, or modeling-based research that will contribute to progress in the field, develop new scientific methods, and apply a known method to a different field. |
Examination |
LO-3 | Can know how to validate laboratory methods. |
PO-1 Develop advanced theoretical and applied knowledge in the field, depending on undergraduate and graduate qualifications. PO-2 Can make connections between different disciplines and sub-fields that their field is related to by using their expert knowledge and skills, work in harmony in research groups. PO-3 Can closely follow national and international developments in the field of chemistry. PO-4 Can systematically follow up-to-date information in the field. PO-7 Can develop new ideas and methods with different perspectives by using high-level competencies such as suggesting solutions to problems that arise in the field and making decisions. PO-8 Can design theoretical, experimental, or modeling-based research that will contribute to progress in the field, develop new scientific methods, and apply a known method to a different field. |
Examination |
LO-4 | Can give extensive information about statistical methods and rules necessary for the correct expression of analysis results. |
PO-1 Develop advanced theoretical and applied knowledge in the field, depending on undergraduate and graduate qualifications. PO-2 Can make connections between different disciplines and sub-fields that their field is related to by using their expert knowledge and skills, work in harmony in research groups. PO-3 Can closely follow national and international developments in the field of chemistry. PO-4 Can systematically follow up-to-date information in the field. PO-6 Can has a scientific and professional ethical understanding and can defend this understanding in any environment. PO-7 Can develop new ideas and methods with different perspectives by using high-level competencies such as suggesting solutions to problems that arise in the field and making decisions. PO-8 Can design theoretical, experimental, or modeling-based research that will contribute to progress in the field, develop new scientific methods, and apply a known method to a different field. PO-9 Can produce solutions to social, scientific, and ethical issues by combining their own knowledge and perspective with up-to-date information about their field. |
Examination |
PO: Programme Outcomes MME:Method of measurement & Evaluation |
Course Contents | ||
The content of this course includes chemical measurement, method validation, accreditation, preparation of the validation report and sample applications. | ||
Weekly Course Content | ||
Week | Subject | Learning Activities and Teaching Methods |
1 | Chemical Measurement purpose and parameters affecting the measurement result | |
2 | Reliable analysis conditions, laboratory accreditation | |
3 | Method validation and its importance | |
4 | Analytical method validation parameters | |
5 | Reference materials | |
6 | Internal quality control, external quality control | |
7 | Analytical method validation study design | |
8 | mid-term exam | |
9 | Preparation of the validation report | |
10 | Measurement uncertainty and sources of uncertainty | |
11 | Application examples | |
12 | Application examples | |
13 | Application examples | |
14 | Application examples | |
15 | Evaluations | |
16 | final exam | |
Recommend Course Book / Supplementary Book/Reading | ||
1 | Skoog, D. A., West D. M., Holler, F. J. (Kılıç, E, Köseoğlu, F. (Ed.)) (1996). Analitik Kimya Temelleri, 7. Baskı. Ankara: Bilim Yayıncılık | |
Required Course instruments and materials | ||
Theoretical lectures, student seminars and article review studies will be carried out. |
Assessment Methods | |||
Type of Assessment | Week | Hours | Weight(%) |
mid-term exam | 8 | 1 | 40 |
Other assessment methods | |||
1.Oral Examination | |||
2.Quiz | |||
3.Laboratory exam | |||
4.Presentation | |||
5.Report | |||
6.Workshop | |||
7.Performance Project | |||
8.Term Paper | |||
9.Project | |||
final exam | 16 | 1 | 60 |
Student Work Load | |||
Type of Work | Weekly Hours | Number of Weeks | Work Load |
Weekly Course Hours (Theoretical+Practice) | 3 | 14 | 42 |
Outside Class | |||
a) Reading | 4 | 8 | 32 |
b) Search in internet/Library | 4 | 8 | 32 |
c) Performance Project | 0 | ||
d) Prepare a workshop/Presentation/Report | 0 | ||
e) Term paper/Project | 0 | ||
Oral Examination | 0 | ||
Quiz | 0 | ||
Laboratory exam | 0 | ||
Own study for mid-term exam | 4 | 8 | 32 |
mid-term exam | 1 | 1 | 1 |
Own study for final exam | 5 | 8 | 40 |
final exam | 1 | 1 | 1 |
0 | |||
0 | |||
Total work load; | 180 |