|
|||||
| Year/Semester of Study | 1 / Fall Semester | ||||
| Level of Course | 3rd Cycle Degree Programme | ||||
| Type of Course | Optional | ||||
| Department | TEKLİF EDİLEN KIMYA (DOKTORA) | ||||
| Pre-requisities and Co-requisites | None | ||||
| Mode of Delivery | Face to Face | ||||
| Teaching Period | 14 Weeks | ||||
| Name of Lecturer | ASLIHAN UZUN (akaratepe@nevsehir.edu.tr) | ||||
| Name of Lecturer(s) | |||||
| Language of Instruction | Turkish | ||||
| Work Placement(s) | None | ||||
| Objectives of the Course | |||||
| The aim of this course is to teach students information about proving the suitability of a method or measurement procedure for the purposes determined with written evidence by objective testing. | |||||
| Learning Outcomes | PO | MME | |
| The students who succeeded in this course: | |||
| LO-1 | Can know what method validation is and why it is needed. |
PO-1 Develop advanced theoretical and applied knowledge in the field, depending on undergraduate and graduate qualifications. PO-3 Can closely follow national and international developments in the field of chemistry. PO-4 Can systematically follow up-to-date information in the field. PO-6 Can has a scientific and professional ethical understanding and can defend this understanding in any environment. PO-7 Can develop new ideas and methods with different perspectives by using high-level competencies such as suggesting solutions to problems that arise in the field and making decisions. PO-8 Can design theoretical, experimental, or modeling-based research that will contribute to progress in the field, develop new scientific methods, and apply a known method to a different field. PO-9 Can produce solutions to social, scientific, and ethical issues by combining their own knowledge and perspective with up-to-date information about their field. |
Examination |
| LO-2 | Can know the parameters used in method validation. |
PO-1 Develop advanced theoretical and applied knowledge in the field, depending on undergraduate and graduate qualifications. PO-2 Can make connections between different disciplines and sub-fields that their field is related to by using their expert knowledge and skills, work in harmony in research groups. PO-3 Can closely follow national and international developments in the field of chemistry. PO-4 Can systematically follow up-to-date information in the field. PO-7 Can develop new ideas and methods with different perspectives by using high-level competencies such as suggesting solutions to problems that arise in the field and making decisions. PO-8 Can design theoretical, experimental, or modeling-based research that will contribute to progress in the field, develop new scientific methods, and apply a known method to a different field. |
Examination |
| LO-3 | Can know how to validate laboratory methods. |
PO-1 Develop advanced theoretical and applied knowledge in the field, depending on undergraduate and graduate qualifications. PO-2 Can make connections between different disciplines and sub-fields that their field is related to by using their expert knowledge and skills, work in harmony in research groups. PO-3 Can closely follow national and international developments in the field of chemistry. PO-4 Can systematically follow up-to-date information in the field. PO-7 Can develop new ideas and methods with different perspectives by using high-level competencies such as suggesting solutions to problems that arise in the field and making decisions. PO-8 Can design theoretical, experimental, or modeling-based research that will contribute to progress in the field, develop new scientific methods, and apply a known method to a different field. |
Examination |
| LO-4 | Can give extensive information about statistical methods and rules necessary for the correct expression of analysis results. |
PO-1 Develop advanced theoretical and applied knowledge in the field, depending on undergraduate and graduate qualifications. PO-2 Can make connections between different disciplines and sub-fields that their field is related to by using their expert knowledge and skills, work in harmony in research groups. PO-3 Can closely follow national and international developments in the field of chemistry. PO-4 Can systematically follow up-to-date information in the field. PO-6 Can has a scientific and professional ethical understanding and can defend this understanding in any environment. PO-7 Can develop new ideas and methods with different perspectives by using high-level competencies such as suggesting solutions to problems that arise in the field and making decisions. PO-8 Can design theoretical, experimental, or modeling-based research that will contribute to progress in the field, develop new scientific methods, and apply a known method to a different field. PO-9 Can produce solutions to social, scientific, and ethical issues by combining their own knowledge and perspective with up-to-date information about their field. |
Examination |
| PO: Programme Outcomes MME:Method of measurement & Evaluation |
|||
| Course Contents | ||
| The content of this course includes chemical measurement, method validation, accreditation, preparation of the validation report and sample applications. | ||
| Weekly Course Content | ||
| Week | Subject | Learning Activities and Teaching Methods |
| 1 | Chemical Measurement purpose and parameters affecting the measurement result | |
| 2 | Reliable analysis conditions, laboratory accreditation | |
| 3 | Method validation and its importance | |
| 4 | Analytical method validation parameters | |
| 5 | Reference materials | |
| 6 | Internal quality control, external quality control | |
| 7 | Analytical method validation study design | |
| 8 | mid-term exam | |
| 9 | Preparation of the validation report | |
| 10 | Measurement uncertainty and sources of uncertainty | |
| 11 | Application examples | |
| 12 | Application examples | |
| 13 | Application examples | |
| 14 | Application examples | |
| 15 | Evaluations | |
| 16 | final exam | |
| Recommend Course Book / Supplementary Book/Reading | ||
| 1 | Skoog, D. A., West D. M., Holler, F. J. (Kılıç, E, Köseoğlu, F. (Ed.)) (1996). Analitik Kimya Temelleri, 7. Baskı. Ankara: Bilim Yayıncılık | |
| Required Course instruments and materials | ||
| Theoretical lectures, student seminars and article review studies will be carried out. | ||
| Assessment Methods | |||
| Type of Assessment | Week | Hours | Weight(%) |
| mid-term exam | 8 | 1 | 40 |
| Other assessment methods | |||
| 1.Oral Examination | |||
| 2.Quiz | |||
| 3.Laboratory exam | |||
| 4.Presentation | |||
| 5.Report | |||
| 6.Workshop | |||
| 7.Performance Project | |||
| 8.Term Paper | |||
| 9.Project | |||
| final exam | 16 | 1 | 60 |
| Student Work Load | |||
| Type of Work | Weekly Hours | Number of Weeks | Work Load |
| Weekly Course Hours (Theoretical+Practice) | 3 | 14 | 42 |
| Outside Class | |||
| a) Reading | 4 | 8 | 32 |
| b) Search in internet/Library | 4 | 8 | 32 |
| c) Performance Project | 0 | ||
| d) Prepare a workshop/Presentation/Report | 0 | ||
| e) Term paper/Project | 0 | ||
| Oral Examination | 0 | ||
| Quiz | 0 | ||
| Laboratory exam | 0 | ||
| Own study for mid-term exam | 4 | 8 | 32 |
| mid-term exam | 1 | 1 | 1 |
| Own study for final exam | 5 | 8 | 40 |
| final exam | 1 | 1 | 1 |
| 0 | |||
| 0 | |||
| Total work load; | 180 | ||