Nevşehir Hacı Bektaş Veli University Course Catalogue

Information Of Programmes

INSTITUTE OF SCIENCE / KİM603 - TEKLİF EDİLEN KIMYA (DOKTORA)

Code: KİM603 Course Title: ANALYTICAL METHOD VALIDATION Theoretical+Practice: 3+0 ECTS: 6
Year/Semester of Study 1 / Fall Semester
Level of Course 3rd Cycle Degree Programme
Type of Course Optional
Department TEKLİF EDİLEN KIMYA (DOKTORA)
Pre-requisities and Co-requisites None
Mode of Delivery Face to Face
Teaching Period 14 Weeks
Name of Lecturer ASLIHAN UZUN (akaratepe@nevsehir.edu.tr)
Name of Lecturer(s)
Language of Instruction Turkish
Work Placement(s) None
Objectives of the Course
The aim of this course is to teach students information about proving the suitability of a method or measurement procedure for the purposes determined with written evidence by objective testing.

Learning Outcomes PO MME
The students who succeeded in this course:
LO-1 Can know what method validation is and why it is needed. PO-1 Develop advanced theoretical and applied knowledge in the field, depending on undergraduate and graduate qualifications.
PO-3 Can closely follow national and international developments in the field of chemistry.
PO-4 Can systematically follow up-to-date information in the field.
PO-6 Can has a scientific and professional ethical understanding and can defend this understanding in any environment.
PO-7 Can develop new ideas and methods with different perspectives by using high-level competencies such as suggesting solutions to problems that arise in the field and making decisions.
PO-8 Can design theoretical, experimental, or modeling-based research that will contribute to progress in the field, develop new scientific methods, and apply a known method to a different field.
PO-9 Can produce solutions to social, scientific, and ethical issues by combining their own knowledge and perspective with up-to-date information about their field.
Examination
LO-2 Can know the parameters used in method validation. PO-1 Develop advanced theoretical and applied knowledge in the field, depending on undergraduate and graduate qualifications.
PO-2 Can make connections between different disciplines and sub-fields that their field is related to by using their expert knowledge and skills, work in harmony in research groups.
PO-3 Can closely follow national and international developments in the field of chemistry.
PO-4 Can systematically follow up-to-date information in the field.
PO-7 Can develop new ideas and methods with different perspectives by using high-level competencies such as suggesting solutions to problems that arise in the field and making decisions.
PO-8 Can design theoretical, experimental, or modeling-based research that will contribute to progress in the field, develop new scientific methods, and apply a known method to a different field.
Examination
LO-3 Can know how to validate laboratory methods. PO-1 Develop advanced theoretical and applied knowledge in the field, depending on undergraduate and graduate qualifications.
PO-2 Can make connections between different disciplines and sub-fields that their field is related to by using their expert knowledge and skills, work in harmony in research groups.
PO-3 Can closely follow national and international developments in the field of chemistry.
PO-4 Can systematically follow up-to-date information in the field.
PO-7 Can develop new ideas and methods with different perspectives by using high-level competencies such as suggesting solutions to problems that arise in the field and making decisions.
PO-8 Can design theoretical, experimental, or modeling-based research that will contribute to progress in the field, develop new scientific methods, and apply a known method to a different field.
Examination
LO-4 Can give extensive information about statistical methods and rules necessary for the correct expression of analysis results. PO-1 Develop advanced theoretical and applied knowledge in the field, depending on undergraduate and graduate qualifications.
PO-2 Can make connections between different disciplines and sub-fields that their field is related to by using their expert knowledge and skills, work in harmony in research groups.
PO-3 Can closely follow national and international developments in the field of chemistry.
PO-4 Can systematically follow up-to-date information in the field.
PO-6 Can has a scientific and professional ethical understanding and can defend this understanding in any environment.
PO-7 Can develop new ideas and methods with different perspectives by using high-level competencies such as suggesting solutions to problems that arise in the field and making decisions.
PO-8 Can design theoretical, experimental, or modeling-based research that will contribute to progress in the field, develop new scientific methods, and apply a known method to a different field.
PO-9 Can produce solutions to social, scientific, and ethical issues by combining their own knowledge and perspective with up-to-date information about their field.
Examination
PO: Programme Outcomes
MME:Method of measurement & Evaluation

Course Contents
The content of this course includes chemical measurement, method validation, accreditation, preparation of the validation report and sample applications.
Weekly Course Content
Week Subject Learning Activities and Teaching Methods
1 Chemical Measurement purpose and parameters affecting the measurement result
2 Reliable analysis conditions, laboratory accreditation
3 Method validation and its importance
4 Analytical method validation parameters
5 Reference materials
6 Internal quality control, external quality control
7 Analytical method validation study design
8 mid-term exam
9 Preparation of the validation report
10 Measurement uncertainty and sources of uncertainty
11 Application examples
12 Application examples
13 Application examples
14 Application examples
15 Evaluations
16 final exam
Recommend Course Book / Supplementary Book/Reading
1 Skoog, D. A., West D. M., Holler, F. J. (Kılıç, E, Köseoğlu, F. (Ed.)) (1996). Analitik Kimya Temelleri, 7. Baskı. Ankara: Bilim Yayıncılık
Required Course instruments and materials
Theoretical lectures, student seminars and article review studies will be carried out.

Assessment Methods
Type of Assessment Week Hours Weight(%)
mid-term exam 8 1 40
Other assessment methods
1.Oral Examination
2.Quiz
3.Laboratory exam
4.Presentation
5.Report
6.Workshop
7.Performance Project
8.Term Paper
9.Project
final exam 16 1 60

Student Work Load
Type of Work Weekly Hours Number of Weeks Work Load
Weekly Course Hours (Theoretical+Practice) 3 14 42
Outside Class
       a) Reading 4 8 32
       b) Search in internet/Library 4 8 32
       c) Performance Project 0
       d) Prepare a workshop/Presentation/Report 0
       e) Term paper/Project 0
Oral Examination 0
Quiz 0
Laboratory exam 0
Own study for mid-term exam 4 8 32
mid-term exam 1 1 1
Own study for final exam 5 8 40
final exam 1 1 1
0
0
Total work load; 180