Nevşehir Hacı Bektaş Veli University Course Catalogue
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| Year/Semester of Study | 1 / Spring Semester | ||||
| Level of Course | 3rd Cycle Degree Programme | ||||
| Type of Course | Optional | ||||
| Department | TEKLİF EDİLEN KIMYA (DOKTORA) | ||||
| Pre-requisities and Co-requisites | None | ||||
| Mode of Delivery | Face to Face | ||||
| Teaching Period | 14 Weeks | ||||
| Name of Lecturer | FATMA KARİPCİN (fkaripcin@nevsehir.edu.tr) | ||||
| Name of Lecturer(s) | FATMA KARİPCİN, | ||||
| Language of Instruction | Turkish | ||||
| Work Placement(s) | None | ||||
| Objectives of the Course | |||||
| The aim of this course is to provide basic information about nuclear magnetic resonance spectroscopy and to gain knowledge and skills for the analysis of 1H-NMR and 13C-NMR spectra of compounds. | |||||
| Learning Outcomes | PO | MME | |
| The students who succeeded in this course: | |||
| LO-1 | Can explain the concept of resonance, the magnetic properties of the atomic nucleus, the spin quantum numbers of the elements, and the behavior of the atomic nucleus in the magnetic field. |
PO-1 Develop advanced theoretical and applied knowledge in the field, depending on undergraduate and graduate qualifications. PO-4 Can systematically follow up-to-date information in the field. PO-7 Can develop new ideas and methods with different perspectives by using high-level competencies such as suggesting solutions to problems that arise in the field and making decisions. |
Examination |
| LO-2 | Can interpret 1H NMR spectra using chemical shift and spin-spin interaction information. |
PO-1 Develop advanced theoretical and applied knowledge in the field, depending on undergraduate and graduate qualifications. PO-4 Can systematically follow up-to-date information in the field. PO-5 Can have the ability to search literature, make presentations, design and prepare experimental setups, and interpret the relevant results. PO-8 Can design theoretical, experimental, or modeling-based research that will contribute to progress in the field, develop new scientific methods, and apply a known method to a different field. |
Examination |
| LO-3 | Can interpret 13C and other NMR spectra. |
PO-1 Develop advanced theoretical and applied knowledge in the field, depending on undergraduate and graduate qualifications. PO-5 Can have the ability to search literature, make presentations, design and prepare experimental setups, and interpret the relevant results. PO-7 Can develop new ideas and methods with different perspectives by using high-level competencies such as suggesting solutions to problems that arise in the field and making decisions. PO-9 Can produce solutions to social, scientific, and ethical issues by combining their own knowledge and perspective with up-to-date information about their field. |
Examination |
| LO-4 | Can make structure determinations by using NMR spectra. |
PO-1 Develop advanced theoretical and applied knowledge in the field, depending on undergraduate and graduate qualifications. PO-5 Can have the ability to search literature, make presentations, design and prepare experimental setups, and interpret the relevant results. PO-7 Can develop new ideas and methods with different perspectives by using high-level competencies such as suggesting solutions to problems that arise in the field and making decisions. PO-8 Can design theoretical, experimental, or modeling-based research that will contribute to progress in the field, develop new scientific methods, and apply a known method to a different field. |
Examination |
| PO: Programme Outcomes MME:Method of measurement & Evaluation |
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| Course Contents | ||
| Within the scope of this course, general information about NMR spectroscopy, magnetic properties of atomic nuclei, chemical shift and affecting factors, spin-spin interaction, NMR types and spectrum interpretations, and structure determination will be explained. | ||
| Weekly Course Content | ||
| Week | Subject | Learning Activities and Teaching Methods |
| 1 | Use of NMR Spectroscopy in structure determination, general information | Narration Method |
| 2 | Magnetic properties of atomic nuclei, Resonance phenomenon | Narration Method |
| 3 | Resonance conditions, working principle of NMR Spectroscopy | Narration Method |
| 4 | Preparation of samples for NMR measurement, Chemical shift | Narration Method |
| 5 | Factors affecting chemical shift: Effect of electron density, Effect of neighboring groups and atoms | Narration Method |
| 6 | Aromatic ring stream, 1H spectra of aromatic compounds | Narration Method |
| 7 | Spin-spin interactions | Narration Method |
| 8 | mid-term exam | |
| 9 | Second order spectra | Narration Method |
| 10 | Slide reagents, double resonance event | Narration Method |
| 11 | 1H NMR Spectrum Solution | Problem Solving Method |
| 12 | 1H NMR Spectrum solution examples | Problem Solving Method |
| 13 | NMR Spectrum Solutions of 13C and other elements | Problem Solving Method |
| 14 | 13C NMR Spectrum solution examples | Problem Solving Method |
| 15 | Two-dimensional (2D) NMR Spectroscopy | Narration Method |
| 16 | final exam | |
| Recommend Course Book / Supplementary Book/Reading | ||
| 1 | Balcı M. (2005). Basic 1H- and 13C-NMR Spectroscopy, Elsevier. | |
| 2 | Balcı M. (1999). Nükleer Manyetik Rezonans Spektroskopisi, ODTÜ Yayıncılık. | |
| Required Course instruments and materials | ||
| Textbook, presentations, projection | ||
| Assessment Methods | |||
| Type of Assessment | Week | Hours | Weight(%) |
| mid-term exam | 8 | 2.00 | 40 |
| Other assessment methods | |||
| 1.Oral Examination | |||
| 2.Quiz | |||
| 3.Laboratory exam | |||
| 4.Presentation | |||
| 5.Report | |||
| 6.Workshop | |||
| 7.Performance Project | |||
| 8.Term Paper | |||
| 9.Project | |||
| final exam | 16 | 2.00 | 60 |
| Student Work Load | |||
| Type of Work | Weekly Hours | Number of Weeks | Work Load |
| Weekly Course Hours (Theoretical+Practice) | 3 | 14 | 42 |
| Outside Class | |||
| a) Reading | 3 | 13 | 39 |
| b) Search in internet/Library | 2 | 13 | 26 |
| c) Performance Project | 0 | ||
| d) Prepare a workshop/Presentation/Report | 0 | ||
| e) Term paper/Project | 0 | ||
| Oral Examination | 0 | ||
| Quiz | 0 | ||
| Laboratory exam | 0 | ||
| Own study for mid-term exam | 4 | 7 | 28 |
| mid-term exam | 2 | 1 | 2 |
| Own study for final exam | 5 | 7 | 35 |
| final exam | 2 | 4 | 8 |
| 0 | |||
| 0 | |||
| Total work load; | 180 | ||