Nevşehir Hacı Bektaş Veli University Course Catalogue
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| Year/Semester of Study | 1 / Fall Semester | ||||
| Level of Course | 3rd Cycle Degree Programme | ||||
| Type of Course | Optional | ||||
| Department | TEKLİF EDİLEN KIMYA (DOKTORA) | ||||
| Pre-requisities and Co-requisites | None | ||||
| Mode of Delivery | Face to Face | ||||
| Teaching Period | 14 Weeks | ||||
| Name of Lecturer | FATMA KARİPCİN (fkaripcin@nevsehir.edu.tr) | ||||
| Name of Lecturer(s) | FATMA KARİPCİN, | ||||
| Language of Instruction | Turkish | ||||
| Work Placement(s) | None | ||||
| Objectives of the Course | |||||
| The aim of this course is to gain knowledge and skills about the basic methods that can be used in the purification and determination of the purity of a synthetically obtained organic or inorganic compound. | |||||
| Learning Outcomes | PO | MME | |
| The students who succeeded in this course: | |||
| LO-1 | Can explain the purpose and use of the purification process, the pre-treatments used in purification, crystallization, filtration, extraction, etc. purification techniques. |
PO-1 Develop advanced theoretical and applied knowledge in the field, depending on undergraduate and graduate qualifications. PO-5 Can have the ability to search literature, make presentations, design and prepare experimental setups, and interpret the relevant results. PO-7 Can develop new ideas and methods with different perspectives by using high-level competencies such as suggesting solutions to problems that arise in the field and making decisions. PO-8 Can design theoretical, experimental, or modeling-based research that will contribute to progress in the field, develop new scientific methods, and apply a known method to a different field. |
Examination |
| LO-2 | Can decide the methods of controlling its purity and the method of purification during the purification of a substance. |
PO-1 Develop advanced theoretical and applied knowledge in the field, depending on undergraduate and graduate qualifications. PO-5 Can have the ability to search literature, make presentations, design and prepare experimental setups, and interpret the relevant results. PO-7 Can develop new ideas and methods with different perspectives by using high-level competencies such as suggesting solutions to problems that arise in the field and making decisions. PO-8 Can design theoretical, experimental, or modeling-based research that will contribute to progress in the field, develop new scientific methods, and apply a known method to a different field. |
Examination |
| LO-3 | Can make structure analysis by deciding on the methods of determining functional groups. |
PO-1 Develop advanced theoretical and applied knowledge in the field, depending on undergraduate and graduate qualifications. PO-2 Can make connections between different disciplines and sub-fields that their field is related to by using their expert knowledge and skills, work in harmony in research groups. PO-5 Can have the ability to search literature, make presentations, design and prepare experimental setups, and interpret the relevant results. PO-8 Can design theoretical, experimental, or modeling-based research that will contribute to progress in the field, develop new scientific methods, and apply a known method to a different field. |
Examination |
| LO-4 | Can decide which technique to use for which substance by using the basic techniques used in purification and the methods used in the structure analysis of the purified substance. |
PO-1 Develop advanced theoretical and applied knowledge in the field, depending on undergraduate and graduate qualifications. PO-2 Can make connections between different disciplines and sub-fields that their field is related to by using their expert knowledge and skills, work in harmony in research groups. PO-9 Can produce solutions to social, scientific, and ethical issues by combining their own knowledge and perspective with up-to-date information about their field. PO-10 Can propose solutions to the problems that arise in her field and in different disciplines, take initiative in decision-making processes, and lead research groups. PO-11 Can contributes to the progress in the field by transforming the studies in her field into scientific articles and publishing them in national and/or international refereed journals. |
Examination |
| PO: Programme Outcomes MME:Method of measurement & Evaluation |
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| Course Contents | ||
| In this course, pre-treatments used in purification, wet analysis methods, crystallization, filtration, extraction, chromatography, distillation methods used for purification, methods used in the determination of functional groups will be explained. In addition, the structure determination of the purified substances using the methods described in this course will also be discussed. | ||
| Weekly Course Content | ||
| Week | Subject | Learning Activities and Teaching Methods |
| 1 | Purification pretreatments | Narration Method |
| 2 | Wet Analysis Methods | Narration Method |
| 3 | Comparison of Wet Analysis and Instrumental Analysis Methods | Narration Method |
| 4 | Purification by crystallization method and types of crystallization | Narration Method |
| 5 | Use of extraction method in purification | Narration Method |
| 6 | Filtrasyon process and its types | Narration Method |
| 7 | Chromatography and application areas | Narration Method |
| 8 | mid-term exam | |
| 9 | Distillation and application areas | Narration Method |
| 10 | Structure determination by determination of functional groups | Narration Method |
| 11 | Methods for determining functional groups | Narration Method |
| 12 | Separation and purification of mixtures | Narration Method |
| 13 | The elucidation of the structures of purified substances by instrumental analysis | Narration Method |
| 14 | Use of NMR spectroscopy in the structure analysis of purified substances | Narration Method |
| 15 | Use of IR spectroscopy in structure analysis of purified substances and sample solutions | Narration Method |
| 16 | final exam | |
| Recommend Course Book / Supplementary Book/Reading | ||
| 1 | Erdik, E., Obalı, M., Işık, N.Y., Öktemer, A. (2011). Denel Organik Kimya, 7. baskı, Gazi Kitabevi. | |
| 2 | Fessenden, R.J., Fessenden, J.S., Feist, P. (2001). Organic laboratory techniques, Brooks/Cole Thomson Learning, Pacific Grove, CA. | |
| Required Course instruments and materials | ||
| Presentations, projection | ||
| Assessment Methods | |||
| Type of Assessment | Week | Hours | Weight(%) |
| mid-term exam | 8 | 2 | 40 |
| Other assessment methods | |||
| 1.Oral Examination | |||
| 2.Quiz | |||
| 3.Laboratory exam | |||
| 4.Presentation | |||
| 5.Report | |||
| 6.Workshop | |||
| 7.Performance Project | |||
| 8.Term Paper | |||
| 9.Project | |||
| final exam | 16 | 2 | 60 |
| Student Work Load | |||
| Type of Work | Weekly Hours | Number of Weeks | Work Load |
| Weekly Course Hours (Theoretical+Practice) | 3 | 14 | 42 |
| Outside Class | |||
| a) Reading | 3 | 12 | 36 |
| b) Search in internet/Library | 2 | 14 | 28 |
| c) Performance Project | 0 | ||
| d) Prepare a workshop/Presentation/Report | 0 | ||
| e) Term paper/Project | 0 | ||
| Oral Examination | 0 | ||
| Quiz | 0 | ||
| Laboratory exam | 0 | ||
| Own study for mid-term exam | 5 | 7 | 35 |
| mid-term exam | 2 | 1 | 2 |
| Own study for final exam | 5 | 7 | 35 |
| final exam | 2 | 1 | 2 |
| 0 | |||
| 0 | |||
| Total work load; | 180 | ||